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In 1899-1900, Morner and Embden isolated cystine from scleroprotein, marking the identification of sulfur-containing amino acids

The effluent was ionized via ion electrospray in negative mode on a TSQ Quantiva triple-quadrupole mass spectrometry with the following instrument settings: ion spray voltage 2500 V, sheath gas 28, ion transfer tube temperature 325, aux gas 8, and FWHM of 0.7 for both Q1/Q3 resolution

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10.1196/annals.1297.059 Ann N Y Acad Sci